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CAS NO.1779-49-3
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2.Dedication to quality, supply& service.
3. Strictly on selecting raw materials.|
4. Reasonable & competitive price, fast lead time.
5. Sample is available for your evaluation & Formulation development.
6.Faster delivery:Sample order in stock and 3-7 days for bulk production.body p span span span span span
7.We have strong cooperation with DHL,TNT, UPS, FEDEX,EMS. Or you also can choose your own shipping forwarder.
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2) 30 Days Warranty of quality of goods.body p span span span span span
Methyl triphenyl phosphine bromide is a solid phosphonium salt flame retardant. At present, halogenated flame retardants are widely used organic flame retardants with excellent flame retardant properties, but when a fire occurs, halogenated flame retardants will release a lot of smoke and toxic hydrogen halide gas, causing secondary hazards. With the promulgation of the EU RoHs and WEEE directives, the application of organic halogenated flame retardants in electronic and electrical equipment and other fields has been subject to many restrictions. Therefore, the development of efficient halogen-free flame retardants has become a very important topic.
Apply
Methyl triphenyl phosphine bromide can be used as a Wittich reagent for the preparation of alkenes and to increase the carbon number of unsaturated carbon chains. The Ylide precursor of Wittig reaction is widely used in the synthesis of unsaturated bonds in liquid crystal materials. It is also widely used in organic synthesis. It is a good cationic phase conversion catalyst.
preparation
Triphenylphosphine (0.0035mol), ammonium bromide (0.00355mol) and trimethyl orthoformate (1.5ml) were successively added into the two-neck flask, and the stirring agent was added. Reflux was heated at 110℃ for 12 hours. After the reaction is complete, it is cooled to room temperature, vaporized under reduced pressure to remove the solvent, and recrystallized with methylene chloride, ethyl acetate, and petroleum ether. The obtained solid was washed with ethyl acetate and petroleum ether, and the white solid obtained after extraction and filtration was moved to a vacuum oven at 60℃ overnight to dry, and the solid quaternary phosphonium salt flame retardant methyl triphenyl phosphine bromide was obtained.
Chemical property
Methyl triphenyl phosphine bromide appears as a white crystal. Melting point 234-235℃. Uses for organic synthesis.
use
Methyl triphenyl phosphine bromide can be used as a Wittich reagent for the preparation of alkenes and to increase the carbon number of unsaturated carbon chains. The Ylide precursor of Wittig reaction is widely used in the synthesis of unsaturated bonds in liquid crystal materials. It is also widely used in organic synthesis. It is a good cationic phase conversion catalyst.
use
Using Wittig reaction, it is widely used in methylene reaction. Wittig enylation salt, through closed loop metathesis, for the synthesis of an enyne application that can provide a benzodiazine heterocycle system. Wittig enylation salt, recently used in the synthesis of enyne, produces a benzodiazine ring system through a cyclic metathesis reaction. It is widely used in methylenation through Wittig reactions.
Production method
Dissolve 55g of triphenylphosphine in 45ml of dry benzene, cool, then add 28g of pre-cooled bromomethane, seal and place at room temperature for 2d. Then 500ml of hot benzene was mixed with the reaction mixture, the white solid was filtered and dried, and 70g methyltriphenylphosphine bromide was obtained. The yield is 99%.
Package
1. Inner double plastic bags----25kg/Fiber drum (35*35*45cm, GW: 28kg, NW: 25kg);
2. Inner double plastic bags----5kg/Aluminum foil bag (GW: 6.5kg, NW: 5kg).
3. Inner double plastic bags----1kg/Aluminum foil bag (GW: 1.5kg, NW: 1kg).
P.S.: we accept packaging customization.
Delivery
1. Stock products are normally shipping within 3 working days.
2. For rush delivery, please contact our sales team for particular arrangement.
Shipping Details:
1. We ship goods via DHL, Fedex, UPS, TNT, China post, NL Post and other couriers, weight from 10g to 1000kg or even bulker.
2. Shipping details & shipping documents will be provided and sent by email.
3. We keep tracking the shippment until clients well received.
4. After years export shipping experience, with professional and experienced can be delivered in many different ways safely and efficiently.
Our company specializes in processing and selling chemical raw materials, chemical products, pharmaceutical intermediates, veterinary medicine intermediates, dye intermediates, pigments, cosmetics raw materials and chemical reagents,
Our company has a number of sales team, service and information feedback vertical integration of a sound marketing network, products are sold throughout the country and exported to South Asia, Europe, America, Africa and other more than 20 countries and regions.
Companies adhering to the "pursuit of quality, innovation and development" business philosophy, to serve as a foundation, for the survival by the quality, seek development by science and technology, adhere to quilty comes first,fair price,good sense of customer service and responsibility. in the future HEBEI SHENGSUAN CHEMICAL INDUSTRY CO.,LTD will always hold "integrity, innovation" business philosophy, to achieve honesty management, on the way of specialization, internationalization, Keep moving!
Our advantages:
HEBEI SHENGSUAN CHEMICAL INDUSTRY CO.,LTD. is located in xingtai City, Hebei Province, China. It is a biotechnology enterprise engaged in the research, development, production and sales of animal and plant extracts, cosmetics, pharmaceutical raw materials and intermediates. The company has complete experimental facilities. And advanced testing instruments ensure the stability of product quality from all aspects. The company has a complete sales service system, the products are exported to countries all over the world, and have won a good international reputation with excellent quality and excellent service.
The company has been adhering to the basic principles of "integrity, quality, service, and win-win" to serve customers, constantly strict requirements, set goals, and implement win-win development.
1. All inquiries will be replied within 12 hours.
2. Dedication to quality, supply & service.
3. Strictly on selecting raw materials.
4. Reasonable & competitive price, fast lead time.
5. Sample is available for your evaluation & Formulation development.
6. Faster delivery:Sample order in stock and 3-7 days for bulk production.
7. We have strong cooperation with DHL, TNT, UPS, FEDEX, EMS. Or you also can choose your own shipping forwarder.
8. After-Sale Service:
1) International Authorized Third-Party Test For The Products You Demand.
2) 30 Days Warranty of quality of goods.